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Capacitance Meter or LCR

S

shayan

Jan 1, 1970
0
Hello every one, Can i measure the continuous variation(with frequency
above 10 kHz) in the capacitance and dielectric constant of a fine
capacitor with capacitance meters or LCR's? Please introduce me a web
link for these instruments.
 
Q

qrk

Jan 1, 1970
0
Hello every one, Can i measure the continuous variation(with frequency
above 10 kHz) in the capacitance and dielectric constant of a fine
capacitor with capacitance meters or LCR's? Please introduce me a web
link for these instruments.

An equally vague answer to your vague question is us a network
analyzer with an impedance function if you need to measure impedance
over a frequency range. Hewlett Packard (Agilent) makes these. HP4195
and Agilent 4395 come to mind. This will allow you to measure complex
impedance from 10 Hz to 500 MHz with the proper fixturing. Although
the spec sheet says it will measure impedance above 100 kHz, the
analyzer will do impedance measurements below 100 kHz if you use DC
coupled fixtures - at least in the HP4195.
http://www.agilent.com/

Mark
 
W

Winfield Hill

Jan 1, 1970
0
shayan wrote...
Hello every one, Can i measure the continuous variation(with frequency
above 10 kHz) in the capacitance and dielectric constant of a fine
capacitor with capacitance meters or LCR's? Please introduce me a web
link for these instruments.

I have an hp 4275A LCR meter, which measures from 10kHz to 10MHz with
5.5-digit resolution. You will find, as I have, that most capacitors
will not have a significant capacitance variation over most of that
frequency range. If you have in mind a specific part or type of
capacitor, I would be happy to measure it for you.

OTH, there is the issue of dielectric absorption, which affects the
observed value of capacitors at lower frequencies. If the polarizing
voltage is present long enough, "remnant polarization trapped on
dielectric interfaces" adds to the capacitor's value, see AoE pages
220-221. The hp 4274A 5.5-digit LCR meter measures from 100Hz to
100kHz, and is a good instrument to observe this effect.

Both of these hp instruments appear on eBay from time to time, e.g.
http://cgi.ebay.com/ws/eBayISAPI.dll?ViewItem&item=3875144082
http://cgi.ebay.com/ws/eBayISAPI.dll?ViewItem&item=3872211489

For frequencies below 100kHz, capacitance bridges are better suited
for high resolution measurements. For example, the General Radio
1615-A and 1616 bridges have 6 and 12-digit! readout, respectively.
They can be used down to 10Hz, but the maximum bridge-excitation
voltage must be reduced, lowering the achievable resolution. I have
both of these fine, elegant instruments. :<>) A google search will
turn up used-instrument dealers, and they're supposedly still being
produced by IET, http://www.ietlabs.com/Genrad/GenRadtestInstr.html
At least the old GR datasheets are available there for you to read.
Search on 1620 and 1621 precision capacitance-measurement systems.
 
J

John Woodgate

Jan 1, 1970
0
I read in sci.electronics.design that Winfield Hill <hill_a@t_rowland-
I have an hp 4275A LCR meter, which measures from 10kHz to 10MHz with
5.5-digit resolution. You will find, as I have, that most capacitors
will not have a significant capacitance variation over most of that
frequency range.

Do you not find any self-resonance effects, e.g. with a 1 uF, well below
10 MHz?
 
W

Winfield Hill

Jan 1, 1970
0
John Woodgate wrote...
Winfield Hill wrote ...


Do you not find any self-resonance effects, e.g. with a 1 uF, well
below 10 MHz?

Yes, of course, especially if the capacitor's leads are long enough,
but this is easily corrected for. Actually, my hp 4191A RF impedance
analyzer is better suited for complex-impedance measurements; It goes
from 1 to 1000MHz, and has 4.5-digit readout resolution. I'm looking
for a used 4192A (that I can afford) for more flexible measurements
below 1MHz. And a 4194A would be very nice to have as well. <sigh>
 
J

John Woodgate

Jan 1, 1970
0
I read in sci.electronics.design that Winfield Hill <hill_a@t_rowland-
dotties-harvard-dot.s-edu> wrote (in said:
John Woodgate wrote...

Yes, of course, especially if the capacitor's leads are long enough,
but this is easily corrected for.

Ah, but what you find easy, the OP (and many others) would find a mite
(indeed a 'might') difficult.
 
F

Fred Bartoli

Jan 1, 1970
0
Winfield Hill said:
shayan wrote...

I have an hp 4275A LCR meter, which measures from 10kHz to 10MHz with
5.5-digit resolution. You will find, as I have, that most capacitors
will not have a significant capacitance variation over most of that
frequency range. If you have in mind a specific part or type of
capacitor, I would be happy to measure it for you.

OTH, there is the issue of dielectric absorption, which affects the
observed value of capacitors at lower frequencies. If the polarizing
voltage is present long enough, "remnant polarization trapped on
dielectric interfaces" adds to the capacitor's value, see AoE pages
220-221. The hp 4274A 5.5-digit LCR meter measures from 100Hz to
100kHz, and is a good instrument to observe this effect.

Both of these hp instruments appear on eBay from time to time, e.g.
http://cgi.ebay.com/ws/eBayISAPI.dll?ViewItem&item=3875144082
http://cgi.ebay.com/ws/eBayISAPI.dll?ViewItem&item=3872211489

For frequencies below 100kHz, capacitance bridges are better suited
for high resolution measurements. For example, the General Radio
1615-A and 1616 bridges have 6 and 12-digit! readout, respectively.
They can be used down to 10Hz, but the maximum bridge-excitation
voltage must be reduced, lowering the achievable resolution. I have
both of these fine, elegant instruments. :<>) A google search will
turn up used-instrument dealers, and they're supposedly still being
produced by IET, http://www.ietlabs.com/Genrad/GenRadtestInstr.html
At least the old GR datasheets are available there for you to read.
Search on 1620 and 1621 precision capacitance-measurement systems.

IIRC, the hp4275A is a bridge (more precisely an auto balanced bridge), and
I really don't see what could prevent such bridges to give really high
resolution measurements. I even see more reasons for an ABB to be more
accurate than an "ordinary" bridge (note also that I don't know precisely
how the Genrad are build, so... But I guess there's nothing very special
about them. In case yes, I'd be curious if you had a schematics).

For the ABB, as you might recall from some of my previous posts, I'm in the
process of building a VNA that can also be used as an ABB (and also some
other functions that are only pertinent to my use). I've made some small
tests on those ugly solderless breadboards for the detector with my hp3456A
for the measurement section and got really amazing results, given the
ugliness level. I could easily measure the 0.13pf parasitics that's between
two series of contacts separated by a guarding one for example, and also
could easily resolve the fF with good stability.
The expected linearity is on the ppm range and only depends on DC
amplifiers, so can be improved at will (almost).
The final product is expected to be largely as good.

I really can't see what makes you saying this.
 
S

shayan

Jan 1, 1970
0
Hi Win. Tank you for your kindness and answering to my request.
Indeed I'm a chemical engineer and I want to use a special capacitor
for measuring the variation of dielectric constant in a fluidized bed.
A fluidized bed is column in which air or another fluid is entering
from bottom and fluidized the fine particles (5 to 500 micrometer)
exist in the column.
By variation in the particle concentration in the capacitor volume its
dielectric also changed. If we could measure this changing in
dielectric with a high sampling rate, we could calculate the particle
concentration using convenient equations. But the traditional LCR's
have not enough measurement speed (minimum 2 ms) and we want the
sampling frequencies above 5 kHz (measurement speed below 0.2 ms).
By which type of capacitance meters can I do this?
 
F

Fred Bartoli

Jan 1, 1970
0
shayan said:
Hi Win. Tank you for your kindness and answering to my request.
Indeed I'm a chemical engineer and I want to use a special capacitor
for measuring the variation of dielectric constant in a fluidized bed.
A fluidized bed is column in which air or another fluid is entering
from bottom and fluidized the fine particles (5 to 500 micrometer)
exist in the column.
By variation in the particle concentration in the capacitor volume its
dielectric also changed. If we could measure this changing in
dielectric with a high sampling rate, we could calculate the particle
concentration using convenient equations. But the traditional LCR's
have not enough measurement speed (minimum 2 ms) and we want the
sampling frequencies above 5 kHz (measurement speed below 0.2 ms).
By which type of capacitance meters can I do this?

What is your measurement frequency range?
What is your estimated capacitance range?
What is you budget?

Without those values, nobody can help you more than some vague
considerations.
Even orders or magnitude will help.
 
W

Winfield Hill

Jan 1, 1970
0
Fred Bartoli wrote...
IIRC, the hp4275A is a bridge (more precisely an auto balanced bridge),
and I really don't see what could prevent such bridges to give really high
resolution measurements. I even see more reasons for an ABB to be more
accurate than an "ordinary" bridge (note also that I don't know precisely
how the Genrad are build, so... But I guess there's nothing very special
about them. In case yes, I'd be curious if you had a schematics).

In theory the 4275A is a bridge, but quite unlike a conventional bridge
such as the GR instruments. The latter use ratio transformers, and all
four arms of the bridge are apparent, including the reference capacitors.
HP calls the 4275 circuit a "voltage-vector current measurement" method.
A detailed look at the circuit schematic reveals many other components,
although there is a balance resistor and null point. I haven't learned
much about the nature of this balance resistor, which I imagine must not
have any self capacitance. The schematics show five or six components
making up each "resistor." I haven't torn my 4275A apart to examine it.
For the ABB, as you might recall from some of my previous posts, I'm in
the process of building a VNA that can also be used as an ABB (and also
some other functions that are only pertinent to my use). I've made some
small tests on those ugly solderless breadboards for the detector with
my hp3456A for the measurement section and got really amazing results,
given the ugliness level. I could easily measure the 0.13pf parasitics
that's between two series of contacts separated by a guarding one for
example, and also could easily resolve the fF with good stability.

I haven't been following your posts, what were some subject headings?

As for the measurements, yes it's easy to get into the fF territory.
The 4275A measures 0.01fF in its slower high-resolution mode, the same
capability as the GR 1615-A bridge (the GR bridge has the benefit of
allowing one to use an external variable-frequency oscillator). My
own hybrid distance-meter design (ratio transformer + multiplier fine
balance) had even better capability. But GR's 1616 was much better,
with a 0.1aF most-sensitive measuring digit. They literally have a
12-digit readout! I don't think that can be achieved without using
precision low-impedance ratio transformers in an honest-to-god bridge.
The expected linearity is on the ppm range and only depends on DC
amplifiers, so can be improved at will (almost).
The final product is expected to be largely as good.

It would be nice if I understood your circuit.

In the case of the 4275A, highly-linear RF phase-detector multipliers
are necessary, which they implement with JFETs driven from an unusual
staircase waveform circuit that suppresses the 3rd and 5th harmonics.
 
C

Chris

Jan 1, 1970
0
shayan said:
Hi Win. Tank you for your kindness and answering to my request.
Indeed I'm a chemical engineer and I want to use a special capacitor
for measuring the variation of dielectric constant in a fluidized bed.
A fluidized bed is column in which air or another fluid is entering
from bottom and fluidized the fine particles (5 to 500 micrometer)
exist in the column.
By variation in the particle concentration in the capacitor volume its
dielectric also changed. If we could measure this changing in
dielectric with a high sampling rate, we could calculate the particle
concentration using convenient equations. But the traditional LCR's
have not enough measurement speed (minimum 2 ms) and we want the
sampling frequencies above 5 kHz (measurement speed below 0.2 ms).
By which type of capacitance meters can I do this?

Hi, Shayan. Glad to hear from you again. Looking back on my previous
post, I think I was a little impatient with your very brief problem
description, and wasn't sure if it was a legitimate post. Sorry.

But I believe I got the drift of where you're headed. I'm hearing you
saying that you've got two plates suspended in a fluidized bed, and
you're trying to find particle density by measuring capacitance to find
dielectric constant of the fluidized powder between the plates. A
couple of questions come to mind:

* I'm going to assume you've got a fluidized bed with a powder being
fluidized by air (again, your description of your problem leaves
something to be desired -- what's the powder, what's the medium?). If
so, you're depending on the difference between the dielectric constant
of the air and that of the powder to provide you with something you can
measure to infer powder density. Note that unless there's a lot of
difference in the dielectric constant of the air and the powder
('tain't necessarily so), it might be that you are trying to infer more
accuracy than you can get with that type of measurement. If the
dielectric constants are close, the most accurate capacitance
measurement isn't going to help, except in a very rough way. If
there's a more dramatic difference in masses per given volume for
powder and medium than their respective dielectric densities, might it
be better to use a stirrer and measure torque?

* Fluidization usually occurs with mechanical vibration of the bed.
In a system with air bubbles, the mechanical shaking makes the air
bubbles progressively smaller, until the powder/air mix acts like a
liquid. I'm not sure why, in a mechanical system like a fluidized bed,
5,000 measurements per second are desirable. Usually it takes from
tenths of seconds to seconds for the powder and the meduim to
homogenize. Again, a better description might help. This might be an
esoteric application we don't know about.

* This sounds like a fairly small (low pF range) capacitance. From a
production/lab standpoint, if "real-time control" required such speeds,
I might be tempted to cobble together a fairly high speed oscillator
using the capacitance of the plates in the bed (possibly even
suspending the rest of the oscillator in the bed itself), divide it
down to an appropriate range with a comparator and some logic ICs, and
after optocoupling, use a high speed counter board in a PC to collect
and process period data. Either that, or you can use the divided down
optocoupled signal to gate a counter, which would drive a D-to-A
converter. You would infer capacitance from period or analog voltage,
and then infer powder density from the inferred dielectric constant of
the fluidized powder -- after all, your plate size remains the same,
right? This has several advantages. And you'll have your 5KHz data
stream.

I believe that, with reasonable care, you can get much better than 1%
accuracy with this type of system, which might be enough if the
differences in dielectric constants are great enough. It would require
some cobbling, but might cost significantly less than your instrument,
and might be a lot more reliable in a production/lab environment.

By the way, you should watch for the development of static charge in
the fluidized bed, and see if that's going to interfere with your
measurements. You might be able to detect this by putting a high
impedance voltmeter on your measurement plates with nothing attached,
and monitoring to see if any charge is developed. Also, if you're
using an air bed, you want to get a good handle on humidity issues,
because that will seriously affect your measurements, as well as
possibly affecting your process. Fluidized beds are a battle to get
running well, and usually something of a mess. By the way, I'm sure it
really isn't necessary to mention this, but from my experience, make
sure everyone's read the MSDS and uses adequate breathing protection
where necessary. Lab/machine operators sometimes don't follow even the
best instructions.

Thanks for posting again, and putting up with some unjustified
impatience on my earlier post. I'd like to hear any additional details
or project requirements.

Chris
 
W

Winfield Hill

Jan 1, 1970
0
shayan wrote...
Hi Win. Tank you for your kindness and answering to my request.
Indeed I'm a chemical engineer and I want to use a special capacitor
for measuring the variation of dielectric constant in a fluidized bed.
A fluidized bed is column in which air or another fluid is entering
from bottom and fluidized the fine particles (5 to 500 micrometer)
exist in the column.
By variation in the particle concentration in the capacitor volume
its dielectric also changed. If we could measure this changing in
dielectric with a high sampling rate, we could calculate the particle
concentration using convenient equations. But the traditional LCR's
have not enough measurement speed (minimum 2 ms) and we want the
sampling frequencies above 5 kHz (measurement speed below 0.2 ms).
By which type of capacitance meters can I do this?

I'm not aware of any that any that fast, although that's likely my
own ignorance. I'm puzzled by your need for a 5kHz sampling rate,
are you trying to measure turbulence dissipation or something, with
a very small cell? You can make an LC oscillator that's running at
several MHz (so its frequency changes within 200us, keeping a high
resonance Q in mind), and take rapid measurements with a vernier-
interpolation period counter. Period counting is normally limited
in resolution, but the vernier-interpolation technique solves this
problem for short measurements. See AoE pages 1020 to 1024, where
we mention the hp5370B counter and describe how it works. According
to the datasheet, the 5370B can take 8000 sustained measurements/sec.
The 5370B went for $12,100 in my 1989 catalog, but I got one on eBay
at a much lower price. Another counter with high-speed capability
is the Stanford Research SR620, which can do 1400 measurements/sec.
http://www.srsys.com/products/SR620.htm Costs about $5000.
 
S

shayan

Jan 1, 1970
0
Measurement frequency: minimum 5kHz

Estimated capacitance: .001pF - 1mF

Budget: maximum 5k$
 
W

Winfield Hill

Jan 1, 1970
0
shayan wrote...
Measurement frequency: minimum 5kHz

Does this mean 5000 meas/sec, or does it mean a 5kHz
ac measurement frequency?
 
S

shayan

Jan 1, 1970
0
We need the sampling frequency( =measurement frequency) above 5000
sample per second

Regards
Shayan
 
W

Winfield Hill

Jan 1, 1970
0
Winfield Hill wrote...
shayan wrote...

I'm not aware of any that any that fast, although that's likely my
own ignorance. I'm puzzled by your need for a 5kHz sampling rate,
are you trying to measure turbulence dissipation or something, with
a very small cell? You can make an LC oscillator that's running at
several MHz (so its frequency changes within 200us, keeping a high
resonance Q in mind), and take rapid measurements with a vernier-
interpolation period counter. Period counting is normally limited
in resolution, but the vernier-interpolation technique solves this
problem for short measurements. See AoE pages 1020 to 1024, where
we mention the hp5370B counter and describe how it works. According
to the datasheet, the 5370B can take 8000 sustained measurements/sec.
The 5370B went for $12,100 in my 1989 catalog, but I got one on eBay
at a much lower price. Another counter with high-speed capability
is the Stanford Research SR620, which can do 1400 measurements/sec.
http://www.srsys.com/products/SR620.htm Costs about $5000.

An hp 5370B reciprocal interpolating counter is up on eBay, $850.
http://cgi.ebay.com/ws/eBayISAPI.dll?ViewItem&item=3878318616
 
F

Fred Bartoli

Jan 1, 1970
0
Winfield Hill said:
Fred Bartoli wrote...

In theory the 4275A is a bridge, but quite unlike a conventional bridge
such as the GR instruments. The latter use ratio transformers, and all
four arms of the bridge are apparent, including the reference capacitors.
HP calls the 4275 circuit a "voltage-vector current measurement" method.
A detailed look at the circuit schematic reveals many other components,
although there is a balance resistor and null point. I haven't learned
much about the nature of this balance resistor, which I imagine must not
have any self capacitance. The schematics show five or six components
making up each "resistor." I haven't torn my 4275A apart to examine it.

Yes, this resistance is a critical component (if you want some bandwidth)
and this is a pb I haven't thought about yet. Thanks for having given the
begining of a solution.

I haven't been following your posts, what were some subject headings?

Nothing very exciting I suppose. The post were about some detail points.
Most are there, I guess :
http://groups-beta.google.com/groups?q=bartoli+vna


As for the measurements, yes it's easy to get into the fF territory.
The 4275A measures 0.01fF in its slower high-resolution mode, the same
capability as the GR 1615-A bridge (the GR bridge has the benefit of
allowing one to use an external variable-frequency oscillator). My
own hybrid distance-meter design (ratio transformer + multiplier fine
balance) had even better capability. But GR's 1616 was much better,
with a 0.1aF most-sensitive measuring digit. They literally have a
12-digit readout! I don't think that can be achieved without using
precision low-impedance ratio transformers in an honest-to-god bridge.

Hmm, not so sure. What you need is a sensitive vector measurement, and a
null tuning mean. This will give you "coarse" nulling. Then you boos the
detector gain to precisely measure the remaining unnulled component at the
nulling node(s) and some math will give you the extra digits through ako
precision virtual nulling. If you have a sensitive enough and linear enough
detector, the figure can be astonishing and, I think, will compensate for
not having standards to switch.
I don't have the GR1616 manual but have found the 1615 one. The detector is
(obviously) only for nulling, and all the sensitivity comes from the dynamic
range given by the switched standards and the ratio transformer. Furthermore
the vector measurement capability allow for noise averaging which the
magnitude null detector can't provide.

Another thing to consider is that the ratio transformer bridges are rather
bandwidth limited.

It would be nice if I understood your circuit.

I'll email you about this, 'cause I can't disclose it.

In the case of the 4275A, highly-linear RF phase-detector multipliers
are necessary, which they implement with JFETs driven from an unusual
staircase waveform circuit that suppresses the 3rd and 5th harmonics.

Do you really mean that they've implemented the detector at the RF level and
not after an IF amplifier?

Hmm, that could explain a lot of things and that's why I've prefered the
other way (which is possible with todays components and was probably much
more difficult when the hp4275 was designed). Another reason is that I
certainly don't have the same ressources capabilities and I have to cheat a
bit :)
 
F

Fred Bartoli

Jan 1, 1970
0
Winfield Hill said:
Fred Bartoli wrote... component...

The reason a ratio transformer is needed has nothing at all to do with
sensitivity, and everything to do with accuracy, linearity and stability.

That's not what I meant. I was speaking of possibly approaching those
bridges performances (at least the easiest one) with the ABB by using the
fact that I have a highly linear and stable vectorial detector.
If I fell inclined and have some time when I have my two IF/detector boards
debugged, I might try to push the limits and see where we go.
There certainly was no problem implementing a vector IF strip when the
4275 was designed, quite the contrary: Implementing their accurate RF
circuit at 10MHz was definitely a challenge. I'm not sure why they made
their choices, but it's clear they knew what they were doing!

That's not the detection that's causing problem, but rather phase stability
of the IF amplifiers if you want really good accuracy. I've run into such
problems and was very very happy to have really modern opamps to help
solving this issue. I agree that doing the detection at the RF stage might
have been tricky, but having followed the other route I can foresee the
difficulties at the moment it was designed and I guess I understand their
choice.
 
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